搜索到6699篇“ MICROWAVE-ASSISTED“的相关文章
Interaction between the Microwave Plasma Generation and the Saturated Voltage during Microwave Pulse Assisted Ignition in ICE Lean Combustion
2025年
Microwave-assisted ignition(MAI)is a promising technology to improve the ignition stability in internal combustion engines under lean conditions.To investigate the interplay between the microwave pulses and the electrical characteristics of ignition plasma,the high-time-resolved electrical characteristics of MAI are measured based on the discharge voltage and current profiles with microwave power varying from 0 to 1000 W.The effects of microwave pulse on the electrical characteristics in the breakdown and glow discharge phases are discussed respectively.The results show that the microwave-induced-voltage-decline(MIVD)occurs during the glow discharge phase,which originates from the increment of free electrons and the additional microwave field.However,this voltage decline is insignificant in the breakdown phase.Moreover,as the free electron number reaches a critical value,a shining plasma can be observed between the gap of electrodes and the voltage decline is stabilized to a"saturated voltage curve".Ultimately,the effect of microwave plasma on the enhancement of ignition kernel area is explored.The result indicates that the enhancement effect increases with plasma duration rising.Those enhancements of earlier-generated plasmas are more significant than those of subsequent plasmas due to the distance limit of the plasma propulsive effect.
SUN WeiCUI YiSONG DaweiTONG ZongpengWU HuiminWANG Zhaowen
Microwave-assisted dehydration of strontium hydroxide octahydrate:Experimental study and kinetic modeling analysis
2025年
In this context,the present study proposes the use of microwave irradiation to improve the dehydration rate and efficiency of strontium hydroxide octahydrate(Sr(OH)_(2)·8H_(2)O)without introducing contaminants.This study revealed that the use of microwave irradiation to dehydrate Sr(OH)_(2)·8H_(2)O is feasible and surprisingly efficient.The effects of this approach on important parameters were investigated using response surface methodology(RSM).The results revealed that the microwave dehydration process follows a linear polynomial model.In addition,compared with the heating time and material thickness,the microwave-assisted dehydration of Sr(OH)_(2)·8H_(2)O is sensitive to the microwave power and not to the material mass.The relative dehydration percentage reached 99.99%when heated in a microwave oven at 950Wfor just 3 min.In contrast,a relative dehydration percentage of 94.6%was reached when heated in an electric furnace at 180℃for 120 min.The XRD spectra also revealed that most of the Sr(OH)_(2)·8H_(2)O transformed into Sr(OH)_(2)after dehydration via microwave irradiation,whereas a significant portion of the Sr(OH)_(2)·H_(2)O remained after conventional electric dehydration.The experimental data were fitted and analyzed via the thin-layer drying dynamics model,and the results indicated that the dehydrating behavior of Sr(OH)_(2)·8H_(2)O could be well described by the Page model.
Wankun WangFuchun Wang
关键词:DEHYDRATIONKINETICMICROWAVE
Microwave-Assisted Acetylated Lignin Loaded into Cellulose Acetate for Efficient UV-Shielding Films
2025年
Developing favorable bio-based polymers that replace petroleum-based plastics is an essential environmental demand.Lignin is a by-product of the chemical pulping industry.It is a natural UV protection ingredient in broad-spectrum(UVA and UVB)sunscreens.It could be partially and selectively acetylated in a simple,fast,and more reliable process.In this work,a composite film was prepared with UV-resistant properties through a casting method.Bio-based cellulose acetate(CA)was employed as a major matrix while nano-acetylated kraft lignin(AL-NPs)was used as filler during synthesizing UV-shielding films loaded with various amounts(1–5 wt.%)of AL-NPs.Kraft lignin was acetylated through a simple and fast microwave-assisted process using acetic acid as a solvent and acetylating agent.The physicochemical and morphological characteristics of the prepared films were evaluated using different methods,including scanning electron microscopy(SEM),Fourier Transform Infrared Spectroscopy(FTIR),X-ray diffraction analysis(XRD),mechanical testing and contact angle measurement.The UV-Vis spectroscopy optical investigation of the prepared films revealed that AL-NPs in the CA matrix showed strong UV absorption.This feature demonstrated the effectiveness of our research in developing UV-resistant bio-based polymer films.Hence,the prepared films can be considered as successful candidates to be applied in packaging applications.
Ahmed M.KhalilSamir Kamel
关键词:UV-SHIELDING
微波辅助低共熔溶剂合成3,5-二苯基吡啶
2025年
以苯乙醛为原料、乙酸铵为氮源,采用微波辅助低共熔溶剂法合成了3,5-二苯基吡啶,对其合成条件进行了优化,并通过^(1)HNMR、^(13)CNMR、EI-MS对其结构进行了表征。结果表明,3,5-二苯基吡啶的最优合成条件如下:苯乙醛用量为1.0 mmol、乙酸铵用量为1.2 mmol、以氯化胆碱-乙二醇(物质的量比1∶1)为低共熔溶剂、反应时间为90 s、微波功率为240 W,在此条件下,3,5-二苯基吡啶收率可达80.61%。
闫浩胡梦周小强田杨锴王新颜
关键词:苯乙醛微波辅助
微波辅助提取松乳菇多糖及其抗氧化性研究
2025年
以松乳菇(Lactarius deliciosus)为原材料,选取料液比、微波功率、微波时间、水浴温度、水浴时间5个变量进行单因素试验,利用响应面分析对微波辅助提取松乳菇多糖工艺进行优化,并对其抗氧化性进行研究。结果表明,最佳提取工艺条件为料液比1∶35 g/mL、微波功率640 W、微波时间25 s、水浴温度90℃、水浴时间120 min,在该条件下松乳菇多糖的提取率可达(4.61±0.03)%;松乳菇多糖具有良好的抗氧化性,当松乳菇多糖的质量浓度为1.0 mg/mL时,其总还原能力和DPPH自由基清除率达到最大。
江舒郑玉凤吴芳张锦凡熊佳怡胡婷
关键词:微波辅助提取多糖抗氧化活性
微波辅助萃取油松松针精油的工艺优化及抗氧化活性研究
2025年
目的:优化油松松针精油的最佳萃取工艺,并对油松松针精油进行成分分析、抗氧化研究。方法:以响应面法优化微波辅助萃取(Microwave-assisted extraction,MAE)提取油松松针精油的工艺,利用气相色谱-质谱联用仪(Gaschromatography-mass spectrometry,GC-MS)对萃取的松针精油进行成分检测,并以DPPH、ABTS^(+)自由基清除能力为指标探究其抗氧化活性。结果:最佳萃取工艺为:萃取时间55 min、微波功率550 W、液料比10:1 mL/g,得率预测值0.245%,优化工艺验证结果为0.238%。从精油中得到的候选化合物共104种,其主要成分有桑贝醇(3.938%)、[1R-(1R^(*), 3E,7E,11R^(*),12R^(*))]-4,8,12,15,15-五甲基[9.3.1]十五碳-3,7-二烯-12-醇(3.597%)等。抗氧化实验中以L-抗坏血酸为对照,测定其DPPH和ABTS^(+)自由基清除能力,其半抑制浓度(Half maximal inhibitory concentration,IC_(50))分别为101.74和12.39 mg/mL。松针精油浓度为128.00 mg/mL时,DPPH自由基清除率可达64.92%,ABTS^(+)自由基清除率可达84.11%。结论:通过优化微波辅助萃取油松松针精油的工艺,并测定该方法获得的松针精油的主要挥发性成分,证实其抗氧化活性,为开发松针精油绿色高效提取方法及进一步利用松针精油资源提供了理论支持。
吕素媛商冰清孙璐颜刘国龙赵发梁秀清吴秋耿越
关键词:油松微波辅助萃取抗氧化
微波辅助重瓣蜀葵种子油提取及脂肪酸成分分析
2025年
以石油醚为溶剂,利用微波辅助提取重瓣蜀葵种子油,通过单因素和正交实验优化提取条件,测定了种子油的理化性质,并经甲酯化后测定其脂肪酸成分。研究表明,重瓣蜀葵种子油提取最佳条件为:料液比1∶15、微波功率260 W、微波时间30 min、微波温度40℃,在此条件下重瓣蜀葵种子油的出油率可达到18.77%,其脂肪酸值、皂化值、过氧化值、碘值、密度分别为0.98 mg KOH/g、267.98 mg/g、0.89 mmol/kg、134.43 g/100 g、0.907 g/cm^(3),色泽为浅棕色。经气相色谱仪检测,重瓣蜀葵种子的脂肪酸有11种,主要组成是亚油酸(质量分数为62.45%)、棕榈酸(质量分数为12.77%)、油酸(质量分数为8.45%)、硬脂酸(质量分数为8.37%)等,不饱和脂肪酸质量分数达到72.77%,饱和脂肪酸质量分数达到27.23%。重瓣蜀葵种子油中含有花生二烯酸、花生四烯酸、花生五烯酸和二十二碳六烯酸,有独特的生理作用,具有开发功能性保健植物油的优势,而普通蜀葵种子油中没有检测到,重瓣蜀葵的种子脂肪酸成分发生了变异。
钟姿健姜红宇黄光文桂晨卢子慧陈小明
关键词:种子油微波辅助气相色谱法脂肪酸成分
微波辅助提取GC-MS/MS测定复杂基质底泥中德克隆类化合物及处理效果初探
2025年
德克隆类物质在污泥样品中以痕量水平(ng/g级)存在,加之污泥基质复杂,对污泥中德克隆类化合物的分析带来极大挑战。鉴于此,本文建立了微波辅助提取与气相色谱-三重四极杆串联质谱(GC-MS/MS)相结合,测定污水处理厂底泥中德克隆类化合物的分析方法。底泥样品采用微波辅助提取在线净化的方法,以丙酮-正己烷(1∶1,V/V)作为提取溶剂,在120℃温度和1500W功率条件下,该方法能够高效地从基质复杂的底泥样品中提取出德克隆类化合物,提取回收率超过80%。样品提取后,利用石墨化碳黑(GCB)和乙二胺基-N-丙基(PSA)固相萃取柱进一步净化,可有效地去除色素、脂类和非极性干扰物,减少基质干扰。借助质谱多反应监测(MRM)模式,针对目标化合物的特定离子对进行选择性监测,排除其他干扰离子的影响,从而实现了对德克隆类化合物的准确定量。该方法在5~400ng/mL浓度范围内线性关系良好,相关系数(r)不小于0.998,检出限为0.017~0.040ng/g。在低、中、高三个浓度水平底泥基质中,德克隆类化合物的平均回收率分别为79.8%~99.5%、86.2%~104.8%、91.2%~106.1%,相对标准偏差(RSD)<7%。将该方法应用于实际底泥样品的检测,在11个污水处理厂底泥中均检出德克隆类化合物,且含量较高(31.4~195.6ng/g)。底泥中顺式德克隆(syn-DP)异构体比例的平均值f_(syn)=0.27,低于德克隆(DP)产品的f_(syn)值,这是由于底泥对反式德克隆(anti-DP)的吸附性更强,或底泥中的顺式德克隆(syn-DP)优先发生了生物降解。初步比较了11个污水处理厂采用不同的污水处理工艺处理底泥中德克隆化合物的效果,与活性污泥法水处理相比,采用A2/O工艺处理的德克隆类化合物的浓度显著降低,f_(syn)值显著增高,但其影响机制仍待深入探究。
朱帅沈亚婷沈亚婷潘萌贾静杨志鹏曹建华
关键词:微波辅助提取
微波在离子色谱法测定难溶磷矿中氟和氯的应用
2025年
磷矿石有一些种类难以被酸溶解完全(伴生矿的不同),例如:磷钇矿、硫磷铝锶矿等,标准SN/T2993—2011《磷矿石中氟和氯的测定》规定,用一定体积的稀硫酸溶液在蒸馏装置中消解同时蒸馏用离子色谱仪测定,但难溶的磷矿石基体中的氟氯消解不完全。尝试用微波作用少量硫酸溶液短时间消解完全,放入蒸馏装置加入剩余体积的硫酸溶液蒸馏分离出氟氯离子,此法不使用高温设备,操作简易,与(1)碱熔后用离子选择电极测定结果(GB/T 1872—1995磷矿石和磷精矿中氟含量的测定-离子选择性电极法);(2)碱熔后硫酸酸化蒸馏后再用离子色谱仪测定(SN/T 2993—2011磷矿石中氟和氯的测定)比较,结果和2种方法测定结果无显著性差异,微波消解法加标回收率在92.28%~110.00%之间,氟离子相对标准偏差0.87%,氯离子相对标准偏差1.66%,取得了良好的检测结果,方法简单可靠。
彭桦张江坤朱桂华王正南张朝旺田大明李有华杜雄雁李永林
关键词:微波消解
微波辅助离子液体提取余甘子总黄酮及生物活性分析
2025年
为提高余甘子资源利用率,以余甘子果实为原料,采用离子液体的乙醇溶液为介质,微波辅助对余甘子果实的黄酮类物质进行绿色提取,并进行生物活性分析。以余甘子冻干粉总黄酮含量为评价指标,在优选离子液体种类、浓度及微波提取条件的基础上,利用Box-Behnken响应曲面实验优化出最佳提取条件。结果显示,[BMIM]Cl浓度为0.04 mol/L、料液比为1:10、提取温度为60℃、微波功率为514 W、微波时间为25 min,此条件下,余甘子冻干粉中总黄酮含量为226.38±0.98 mg/g。在测定的浓度范围内,余甘子冻干粉的DPPH(1,1-二苯基-2-苦基肼,C_(18)H_(12)N_(5)O_(6))自由基清除率优于VC,羟自由基清除率低于VC,酪氨酸酶抑制率优于曲酸,有一定的抑菌能力,抑制金黄色葡萄球菌的能力强于对大肠杆菌。
喻冬秀黎晓华方梓烨郭佳丽钟建军谢辉
关键词:离子液体微波生物活性

相关作者

谢鹏
作品数:2被引量:11H指数:1
供职机构:湖南人文科技学院
研究主题:催化 除草剂安全剂 QSAR 谷胱甘肽 酰胺类除草剂
杨振军
作品数:133被引量:32H指数:3
供职机构:北京大学
研究主题:修饰 核酸适配体 类似物 SIRNA 缀合
胡文祥
作品数:194被引量:614H指数:13
供职机构:武汉工程大学化工与制药学院
研究主题:微波催化 微波 微波辐射 NMR 分子
王喆之
作品数:435被引量:2,487H指数:24
供职机构:陕西师范大学
研究主题:丹参 山茱萸 白及 生物信息学分析 GC-MS分析
肖亚萍
作品数:2被引量:0H指数:0
供职机构:西北濒危药材资源开发国家工程实验室
研究主题:DPPH·自由基 微波辅助 总酚 提取工艺优化 MICROWAVE-ASSISTED